World Cup points leader Sarah Sjostrom of Sweden stopped Hungary's Katinka Hosszu's clean sweep of the 100m individual medley by winning in a time of 57.49.
The Swedish star later claimed gold in the 50m free (23.21), while Ronomi Kromowidjojo of the Netherlands finished with a time of 23.46 and Pernille Blume of Denmark completed her race in 23.67.
It's the first time that Hosszu has lost this race since 2017 - she's won it 28 times in a row.
"It is the race. Anything can happen in the race. But I swam my fastest 200m fly of the season. That's OK. I think I am still not good at sprint events," the Hungarian said.
Hozzsu was the winner in the 200m butterfly (2:02.86), beating Zhang Yufei of China (2:03.93) and Alexandra Wenk of Germany (2:08.60).
In other women's events, Reva Foos of Germany was the fastest in the 400m freestyle (4:07.07), Kira Toussaint of the Netherlands won the 50m backstroke (26.04) and Yuliya Efimova of Russia ruled the 200m breaststroke (2:16.05).
Singapore is the seventh and last leg of the Swimming World Cup 2018.
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